I am trying to calculate the LOD/LOQ in Skyline Daily for a panel of small molecules of which I have analyzed a dilution series with replicates as well as blanks. Looking at my calibration curve the best fit seems to be linear in log space for the regression. I have Skyline set to calculate LOD as the blank plus 3 * SD. When I look at the document grid or report all of the LOD and most of the LOQ values are left blank. Why is this and how do I get them to appear? Here is a screen shot of my report and a copy of my Skyline document.