                            INSTRUMENT CONTROL PARAMETERS:    GC-TMS
                            ----------------------------------------

   C:\MSDCHEM\1\METHODS\TMS_LCFA.M
      Mon Nov 22 15:05:25 2021

Control Information
------- -----------

Sample Inlet      :  GC
Injection Source  :  Manual
Mass Spectrometer :  Enabled

Oven
Equilibration Time                           0.5 min
Max Temperature                              450 degrees C
Slow Fan                                     Disabled
Oven Program                                 On
    80 °C for 2 min
#1    then 20 °C/min to 160 °C for 2 min
#2    then 2 °C/min to 200 °C for 0 min
#3    then 10 °C/min to 310 °C for 20 min
Run Time                                     59 min
1 min (Post Run)                             275 °C
Cryo                                         Off

Front Injector
Syringe Size                                 10 µL
Injection Volume                             1 µL
Solvent A Washes (PreInj)                    2
Solvent A Washes (PostInj)                   2
Solvent A Volume                             8 µL
Solvent B Washes (PreInj)                    2
Solvent B Washes (PostInj)                   2
Solvent B Volume                             8 µL
Sample Washes                                1
Sample Wash Volume                           3 µL
Sample Pumps                                 2
Dwell Time (PreInj)                          0 min
Dwell Time (PostInj)                         0 min
Solvent Wash Draw Speed                      300 µL/min
Solvent Wash Dispense Speed                  6000 µL/min
Sample Wash Draw Speed                       300 µL/min
Sample Wash Dispense Speed                   6000 µL/min
Injection Dispense Speed                     300 µL/min
Viscosity Delay                              0 sec
Sample Depth                                 4 mm
Injection Type                               Standard
L1 Airgap                                    0.2 µL

Sample Overlap
Sample overlap is not enabled

Front SS Inlet He
Mode                                         Split
Heater                                       On    250 °C
Pressure                                     On    9.3825 psi
Total Flow                                   On    54 mL/min
Septum Purge Flow                            On    3 mL/min
Gas Saver                                    On    20 mL/min After 3 min
Split Ratio                                  50 :1
Split Flow                                   50 mL/min

Thermal Aux 2 (MSD Transfer Line)
Heater                                       On
Temperature Program                          On
    310 °C for 0 min
Run Time                                     59 min

Column #1
Phenomen ZB-1MS: 2564.36749
100% dimethylpolysiloxane
350 °C: 30 m x 250 µm x 0.25 µm
In: Front SS Inlet He
Out: Vacuum

(Initial)                                    80 °C
Pressure                                     9.3825 psi
Flow                                         1 mL/min
Average Velocity                             36.966 cm/sec
Holdup Time                                  1.3526 min
Flow Program                                 Off
    1 mL/min for 0 min
Run Time                                     59 min
1 min (Post Run)                             0.57353 mL/min

Signals
Signal #1: None

Signal #2: None

Signal #3: Test Plot                         Save Off
                                             50 Hz

Signal #4: Test Plot                         Save Off
                                             50 Hz

                                MS ACQUISITION PARAMETERS


General Information
------- -----------

Tune File                : atune.u
Acquistion Mode          : Scan


MS Information
-- -----------

Solvent Delay            : 5.00 min

EMV Mode                 : Gain Factor
Gain Factor              : 1.00
Resulting EM Voltage     : 1282

[Scan Parameters]

Low Mass                 : 50.0
High Mass                : 550.0
Threshold                : 150
Sample #                 : 2       A/D Samples    4
Plot 2 low mass          : 50.0
Plot 2 high mass         : 550.0

[MSZones]

MS Source                : 230 C   maximum 250 C
MS Quad                  : 150 C   maximum 200 C


                             END OF MS ACQUISITION PARAMETERS


                              TUNE PARAMETERS for SN: US12292A15
                        -----------------------------

 Trace Ion Detection is OFF.

 EMISSION    :      34.610
 ENERGY      :      69.922
 REPELLER    :      34.814
 IONFOCUS    :      90.157
 ENTRANCE_LE :      22.000
 EMVOLTS     :    1352.941
                               Actual EMV  :    1282.35
                               GAIN FACTOR :       1.05
 AMUGAIN     :    1668.000
 AMUOFFSET   :     120.438
 FILAMENT    :       1.000
 DCPOLARITY  :       1.000
 ENTLENSOFFS :      20.078
 MASSGAIN    :    -885.000   
 MASSOFFSET  :     -39.000   

                           END OF TUNE PARAMETERS
                      ------------------------------------



                              END OF INSTRUMENT CONTROL PARAMETERS
                              ------------------------------------
