                  INSTRUMENT CONTROL PARAMETERS:    MSD 5975
                  ------------------------------------------

   D:\MassHunter\GCMS\1\methods\Fattyacids_DB5MS30_SSL_rear.M
      Wed Dec 18 20:53:49 2019

Control Information
------- -----------

Sample Inlet             : GC
Injection Source         : GC ALS
Injection Location:  Rear
Mass Spectrometer        : Enabled


 No Sample Prep method has been assigned to this method.


GC
GC Summary
Run Time                                     23.095 min
Post Run Time                                2 min

Oven
Equilibration Time                           0.5 min
Max Temperature                              325 °C
Maximum Temperature Override                 Disabled
Slow Fan                                     Disabled
Temperature
Setpoint                                     On
(Initial)                                    150 °C
Hold Time                                    2 min
Post Run                                     150 °C
Program
#1 Rate                                      15 °C/min
#1 Value                                     220 °C
#1 Hold Time                                 0 min
#2 Rate                                      7 °C/min
#2 Value                                     300 °C
#2 Hold Time                                 5 min



ALS
ALS Errors                                   Pause for user interaction
Back Injector
Syringe Size                                 5 μL
Injection Volume                             1 μL
Solvent A Washes (PreInj)                    2
Solvent A Washes (PostInj)                   0
Solvent A Volume                             4 μL
Solvent B Washes (PreInj)                    2
Solvent B Washes (PostInj)                   0
Solvent B Volume                             4 μL
Sample Washes                                0
Sample Wash Volume                           4 μL
Sample Pumps                                 2
Dwell Time (PreInj)                          0 min
Dwell Time (PostInj)                         0 min
Solvent Wash Draw Speed                      150 μL/min
Solvent Wash Dispense Speed                  1500 μL/min
Sample Wash Draw Speed                       150 μL/min
Sample Wash Dispense Speed                   1500 μL/min
Injection Dispense Speed                     3000 μL/min
Viscosity Delay                              0 sec
Sample Depth                                 Disabled
Injection Type                               Standard
L1 Airgap                                    0.1 μL
Solvent Wash Mode                            A-A2,B-B2

Sample Overlap
Mode                                         Sample overlap is not enabled


Back SS Inlet He
Mode                                         Splitless
Heater                                       On    300 °C
Pressure                                     On    16.008 psi
Total Flow                                   On    20.4 mL/min
Septum Purge Flow                            On    3 mL/min
Gas Saver                                    On    20 After 2 min mL/min
Purge Flow to Split Vent                     15 mL/min at 0 min

Thermal Aux 2 (MSD Transfer Line)
Temperature
Setpoint                                     On
(Initial)                                    280 °C
Post Run                                     0 °C


Column
Column Outlet Pressure                       0 psi
Column #1
Column Information                           Agilent 19091S-433
HP-5MS  5% Phenyl Methyl Silox               
Temperature Range                            -60 °C—325 °C (325 °C)
Dimensions                                   15 m x 250 μm x 0.25 μm
In                                           Back SS Inlet He
Out                                          MSD 
(Initial)                                    150 °C
Pressure                                     16.008 psi
Flow                                         2.4 mL/min
Average Velocity                             83.366 cm/sec
Holdup Time                                  0.29988 min
Flow
Setpoint                                     On
(Initial)                                    2.4 mL/min
Post Run                                     0.57353 mL/min



Aux EPC 4,5,6
Aux EPC 4 He
                                             ***Excluded from Affecting GC's Readiness State***
Pressure
Setpoint                                     On
(Initial)                                    4 psi
Post Run                                     0 psi


Aux EPC 5 He
                                             ***Excluded from Affecting GC's Readiness State***
Pressure
Setpoint                                     Off
(Initial)                                    0 psi
Post Run                                     0 psi


Aux EPC 6 He
                                             ***Excluded from Affecting GC's Readiness State***
Pressure
Setpoint                                     Off
(Initial)                                    0 psi
Post Run                                     0 psi



Signals
Signal #1:  Test Plot
Description                                  Test Plot
Details                                      
Save                                         Off
Data Rate                                    50 Hz

Signal #2:  Test Plot
Description                                  Test Plot
Details                                      
Save                                         Off
Data Rate                                    50 Hz

Signal #3:  Test Plot
Description                                  Test Plot
Details                                      
Save                                         Off
Data Rate                                    50 Hz

Signal #4:  Test Plot
Description                                  Test Plot
Details                                      
Save                                         Off
Data Rate                                    50 Hz




MS Information
-- -----------


JetClean:	No Cleaning


General Information
------- -----------


Acquisition Mode         : Scan
Solvent Delay (minutes)  : 3
Tune file                : D:\MassHunter\GCMS\1\5975\atune.u
EM Setting mode Gain     : 1.000000

Normal or Fast Scanning  : Normal Scanning
Trace Ion Detection      : On
Run Time (if MS only)    : 650 minutes 

[Scan Parameters]
Start Time               : 3
Low Mass                 : 50
High Mass                : 550
Threshold                : 150
A/D Samples:             : 4


[MSZones]

MS Source                   : 230 C   maximum 250 C
MS Quad                     : 150 C   maximum 200 C

Timed Events
----- ------
Number Events= 0



                     END OF MS ACQUISTION PARAMETERS


                        TUNE PARAMETERS for SN: US10484604
                        ---------------------------------

 Trace Ion Detection is ON.

    34.610   :   EMISSION     
    70.347   :   ENERGY       
    29.241   :   REPELLER     
    90.157   :   IONFOCUS     
    19.000   :   ENTRANCE_LENS
  1305.882   :   EMVOLTS      
                              1482.353  : Actual EMV 
                               0.98   : GAIN FACTOR 
  1718.000   :   AMUGAIN      
   121.875   :   AMUOFFSET    
     1.000   :   FILAMENT     
     0.000   :   DCPOLARITY   
    20.078   :   ENTLENSOFFSET
  -798.000   :  MASSGAIN        
   -33.000   :  MASSOFFSET      

                        END OF TUNE PARAMETERS
                        ----------------------



                      END OF INSTRUMENT CONTROL PARAMETERS
                      ------------------------------------
