                        INSTRUMENT CONTROL PARAMETERS:    MSD
                        -------------------------------------

   D:\!Methods\METHODS_TO_USE\alkanes_QC.M
      Mon Feb 03 12:34:38 2025

Control Information
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Sample Inlet             : GC
Injection Source         : PAL Sampler
Injection Location:  Front
Mass Spectrometer        : Enabled


PAL Sampler
PAL Method Information
Parameters of PAL Cycle 
Air Volume (µl)                              0.7
Pre Clean with Solvent 1 ()                  3
Pre Clean with Solvent 2 ()                  0
% Syringe Fill for Cleaning (%)              80
Pre Clean with Sample ()                     3
Sample Amount for Cleaning (µl)              2
Filling Speed (µl/s)                         5
Volume for Filling Strokes (µl)              2
Filling Strokes ()                           3
Inject to                                    GC Inj1
Injection Speed (µl/s)                       40
Pre Inject Delay (ms)                        500
Post Inject Delay (ms)                       500
Post Clean with Solvent 1 ()                 5
Post Clean with Solvent 2 ()                 5


Injection Volume                             1 µl
Overlap Injection Mode                       No Overlap



 No Sample Prep method has been assigned to this method.


GC
GC Summary
Run Time                                     27 min
Post Run Time                                0 min

Oven
Temperature
Setpoint                                     On
(Initial)                                    70 °C
Hold Time                                    4 min
Post Run                                     50 °C
Program
#1 Rate                                      15 °C/min
#1 Value                                     325 °C
#1 Hold Time                                 6 min


Equilibration Time                           1 min
Max Temperature                              325 °C
Maximum Temperature Override                 Disabled
Slow Fan                                     Disabled

Front SSZ Inlet He
Mode                                         Split
Heater                                       On    300 °C
Pressure                                     On    14.951 psi
Total Flow                                   On    181.2 mL/min
Septum Purge Flow                            Off
Gas Saver                                    On    50 After 5 min mL/min
Split Ratio                                  150 :1
Split Flow                                   180 mL/min
Liner                                        A Liner has not been selected.

Column
Column #1
Flow
Setpoint                                     On
(Initial)                                    1.2 mL/min
Post Run                                     0.57353 mL/min

Column Information                           Agilent 19091S-433
HP-5MS  5% Phenyl Methyl Silox               
Temperature Range                            -60 °C—325 °C (325 °C)
Dimensions                                   30 m x 250 μm x 0.25 μm
Main Segment Heated By                       Oven
Segment inSeg                                Heated By Oven: 2.5 m x 250 μm x 0 μm
Segment outSeg                               Heated By Oven: 3 m x 150 μm x 0 μm
In                                           Front SSZ Inlet He
Out                                          MSD 
(Initial)                                    70 °C
Pressure                                     20.307 psi
Flow                                         1.2 mL/min
Average Velocity                             25.42 cm/sec
Holdup Time                                  2.3275 min
Control Mode                                 Constant Flow

Column Outlet Pressure                       0 psi

Detector Evaluation
Perform Detector Evaluation Test             Off
Signal Selected                              No Signal Selected
Checkout Sample                              NONE


MSD Transfer Line
Temperature
Setpoint                                     On
(Initial)                                    325 °C



Valve 1
Name                                         ?
Type                                         Gas Sampling Valve
GSV Loop Volume                              1 mL
Load Time                                    0.5 min
Inject Time                                  0.5 min

Signals
Signal #1:  Test Plot
Description                                  Test Plot
Save                                         Off
Data Rate                                    50 Hz

Signal #2: 
Description                                  None

Signal #3: 
Description                                  None

Signal #4: 
Description                                  None




MS Information
-- -----------


General Information
------- -----------


Acquisition Mode         : SIM/Scan
Solvent Delay (minutes)  : 4
Tune file                : D:\MassHunter\GCMS\1\5977\ATUNE.U
EM Setting mode Gain     : 5.000000

Number of SIM Groups     : 1
Run Time (if MS only)    : 11.63 minutes 

[Scan Parameters]
Start Time               : 4
Low Mass                 : 50
High Mass                : 450
Threshold                : 0
A/D Samples:             : 4


[SIM Parameters]
Group 1               Group ID                  : alkanes_C7-C30
Resolution                : 0
Group Start Time          : 4
Number of Ions            : 1
Ions
Dwell In Group            :(  Mass,  Dwell) (  Mass,  Dwell)  (  Mass,  Dwell) 
                           (  85.10,100  ) 


[MSZones]

MS Source                   : 230 C   maximum 250 C
MS Quad                     : 150 C   maximum 200 C

Timed Events
----- ------
Number Events= 0



                     END OF MS ACQUISITION PARAMETERS


                        TUNE PARAMETERS for SN: US1932R046
                        ---------------------------------

 Trace Ion Detection is OFF.

    34.593   :   EMISSION     
    70.007   :   ENERGY       
    29.321   :   REPELLER     
    90.331   :   IONFOCUS     
    22.672   :   ENTRANCE_LENS
  1618.934   :   EMVOLTS      
                              2157.8  : Actual EMV 
                              15.00   : GAIN FACTOR 
  2157.000   :   AMUGAIN      
   138.125   :   AMUOFFSET    
     2.000   :   FILAMENT     
     1.000   :   DCPOLARITY   
    15.149   :   ENTLENSOFFSET
     0.000   :   Ion_Body     
     0.000   :   EXTLENS      
  -202.000   :  MASSGAIN        
   -24.000   :  MASSOFFSET      

                        END OF TUNE PARAMETERS
                        ----------------------



                        END OF INSTRUMENT CONTROL PARAMETERS
                        ------------------------------------
